Physicochemical Basis of Pharmacy: Analytical Chemistry 1755-F2-CHAN-J

The lectures are intended to:
- familiarize students with the following topics: stages of the analytical process, development of measurement results, validation of analytical methods, classical analysis methods (gravimetric analysis, titrimetric analysis), spectroscopic methods (UV-Vis spectrophotometry, IR, NMR, flame photometry), electroanalytical methods (potentiometry, polarography, voltammetry, conductometry), chromatographic methods (GC, HPLC, TLC, electrophoresis). The laboratories are designed to:
- familiarize students with classical quantitative analysis, which includes gravimetric analysis, and titration methods - acid-base measurement, complexonometry, redoximetry, and precipitation measurement) and instrumental analysis methods (chromatography - GC, HPLC, TLC; spectrophotometry, spectrofluorimetry, flame photometry, voltammetry, conductometry, potentiometry).

The exercises include solving calculation problems in the field of classical quantitative analysis methods, unit conversion, correct presentation of analysis results, and measurement uncertainty.

The seminars are designed to:
- teach how to use scientific literature in the field of analytical chemistry,
- teach independent problem-solving in the field of analytical chemistry, such as selecting the appropriatechnique, method optimization, instrumental and validation.

Learning outcomes - knowledge

Student knows and understand: W1: the basics of classical quantitative analysis methods, including gravimetric analysis and volumetric analysis (alkacimetry, redoximetry, argentometry, complexonometry) – K_B.W11 W2: the application of classical quantitative analysis methods – K_B.W11 W3: the classification and theoretical foundations of instrumental analytical techniques – K_B.W12 W4: the methodological foundations and application of instrumental techniques, including spectroscopic, electrochemical, chromatographic and mass spectrometry – K_B.W12 W5: and is able to apply the criteria for selecting an instrumental analytical method to perform a specific analytical task - K_B.W13 W6: the definitions of analytical method validation parameters, is able to plan, perform and evaluate the validation process – K_B.W14 W7: the types of solutions and their division according to various criteria (e.g. real solutions, colloidal solutions, suspensions) – K_B.W7

Learning outcomes - skills

The student is able to: U1: optimize and validate a classical method for performing an analytical task – K_B.U6 U2: identify and quantitatively analyze elements and chemical compounds using appropriate classical methods – K_B.U7 U3: select, optimize and validate an instrumental method for performing an analytical task – K_B.U6 U4: perform a quantitative analysis of elements and chemical compounds using appropriate instrumental techniques – K_B.U7 U5: assess the reliability and analytical quality of measurement results using appropriate statistical tools – K_B.U7 U6: perform an analysis of water intended for pharmaceutical purposes using recommended analytical methods – K_B.U5

Learning outcomes - social competencies

K1: Uses objective sources of information - K7 K2: Can formulate conclusions based on own measurements or observations - K8

Teaching methods

Lectures: - informative lecture (conventional), - problem-based lecture, - multimedia presentation Llaboratory: - methods: laboratory, observation, exercise, Tutorials and seminars: - activating and problem-based methods – discussion, - classic problem-based method, - use of the Moodle platform

Expository teaching methods

- participatory lecture
- informative (conventional) lecture
- problem-based lecture

Exploratory teaching methods

- experimental
- practical
- observation
- laboratory

Online teaching methods

- methods developing reflexive thinking
- exchange and discussion methods
- cooperation-based methods

Type of course

compulsory course

Prerequisites

It is necessary to have basic knowledge about the properties of chemical compounds and chemical analysis obtained as part of implementing the program of classes in general and inorganic chemistry. In addition, the student should have acquired knowledge and skills in mathematics and statistics.

Course coordinators

Bogumiła Kupcewicz

Assessment criteria

The rules for passing the subject are active participation in didactic classes and obtaining the appropriate number of points. Laboratories: written tests, analyses - passing requires obtaining 60% of points for analyses and tests.
Tutorials and seminars: written and entrance tests - passing requires 60% of points.
Exam: written exam (two parts) - passing requires obtaining 60% of points in each part.

Practical placement

not applicable

Additional information

Additional information (registration calendar, class conductors, localization and schedules of classes), might be available in the USOSweb system:

Description of 1755-F2-CHAN-J in USOSweb