Analytical Chemistry
1710-F2-CHAN-J
The lectures are intended to:
- familiarize the student with the following topics: stages of the analytical process, development of measurement results, validation of analytical methods, classical analysis methods (gravimetric analysis, titrimetric analysis), spectroscopic methods (UV-Vis spectrophotometry, IR, NMR, flame photometry), electroanalytical methods (potentiometry, polarography, voltammetry, conductometry), chromatographic methods (GC, HPLC, TLC, electrophoresis). The laboratories are designed to:
- familiarize students with classical quantitative analysis, which includes gravimetric analysis, titration methods - acid-base chemistry, complexonometry, redoximetry, precipitation chemistry) and instrumental analysis methods (chromatography - GC, HPLC, TLC; spectrophotometry, spectrofluorimetry, flame photometry, voltammetry, conductometry, potentiometry).
The seminars are designed to:
- teach students how to use scientific literature in the field of analytical chemistry,
- teach independent problem solving in the field of analytical chemistry: selection of the appropriate instrumental technique, optimization and method validation.
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Term 2022/23Z:
The lectures are intended to:
- familiarize the student with the following topics: stages of the analytical process, development of measurement results, validation of analytical methods, classical methods of analysis (gravimetric analysis, titrimetric analysis),
The laboratories are intended to:
- familiarize the student with classical quantitative analysis, which includes gravimetric analysis, titrimetric methods – acid-base measurement, complexometry, redoximetry, precipitation measurement).
The auditorium exercises include:
- solving calculation problems used in classical analytical methods |
Term 2023/24Z:
The lectures are intended to:
- familiarize the student with the following topics: stages of the analytical process, development of measurement results, validation of analytical methods, classical methods of analysis (gravimetric analysis, titrimetric analysis),
The laboratories are intended to:
- familiarize the student with classical quantitative analysis, which includes gravimetric analysis, titrimetric methods – acid-base measurement, complexometry, redoximetry, precipitation measurement).
The auditorium exercises include:
- solving calculation problems used in classical analytical methods |
Term 2024/25Z:
The lectures are intended to:
- familiarize the student with the following topics: stages of the analytical process, development of measurement results, validation of analytical methods, classical methods of analysis (gravimetric analysis, titrimetric analysis),
The laboratories are intended to:
- familiarize the student with classical quantitative analysis, which includes gravimetric analysis, titrimetric methods – acid-base measurement, complexometry, redoximetry, precipitation measurement).
The auditorium exercises include:
- solving calculation problems used in classical analytical methods |
Term 2025/26Z:
The lectures are intended to:
- familiarize the student with the following topics: stages of the analytical process, development of measurement results, validation of analytical methods, classical methods of analysis (gravimetric analysis, titrimetric analysis),
The laboratories are intended to:
- familiarize the student with classical quantitative analysis, which includes gravimetric analysis, titrimetric methods – acid-base measurement, complexometry, redoximetry, precipitation measurement).
The auditorium exercises include:
- solving calculation problems used in classical analytical methods |
Total student workload
1. The workload associated with classes requiring direct participation of academic teachers is:
- participation in lectures: 40 hours,
- participation in exercises: 15 hours,
- participation in laboratories: 90 hours,
- participation in seminars: 15 hours,
- additional opportunity for consultation with persons conducting classes: 12 hours.
- participation in the final exam: 3 hours.
The workload associated with classes requiring direct participation of academic teachers is 175 hours, which corresponds to 7.00 ECTS points.
2. Student workload balance:
- participation in lectures: 40 hours,
- participation in exercises: 15 hours,
- participation in laboratories: 90 hours,
- participation in seminars: 15 hours,
- additional opportunity for consultation with persons conducting classes: 12 hours.
- participation in the final exam: 3 hours.
- preparing and completing notes: 20 hours,
- collecting materials and preparing for classes: 37 hours,
- reading the indicated literature: 18 hours,
- preparing for tests: 25 hours,
- preparing for the exam: 25 hours.
The total student workload is 300 hours, which corresponds to 12.0 ECTS points.
3. Workload related to conducted scientific research: - reading indicated scientific literature: 15 hours,
- participation in lectures (taking into account the methodology of scientific research, research results, studies): 30 hours,
- research and scientific consultations: 12 hours
- participation in classes covered by scientific activity (taking into account the methodology of scientific research, research results, studies): 85 hours,
- preparation for classes covered by scientific activity: 40 hours,
- preparation for crediting in the scope of research and scientific aspects of the subject being implemented: 33 hours.
The total student workload related to conducted scientific research is 215 hours, which corresponds to 8.6 ECTS points.
4. Time required to prepare and participate in the assessment process:
- required repetition of material + preparation for tests and exams + preparation for classes – 25 + 25 + 3 =53 (2.12 ECTS points).
5. Time required to complete the mandatory internship:
not applicable
Learning outcomes - knowledge
W1: Knows the basics of classical quantitative analysis methods, including gravimetric analysis and volumetric analysis (alkacymetry, redoximetry, argentometry, complexometry) – K_B.W11
W2: Knows the application of classical quantitative analysis methods – K_B.W11
W3: Knows the classification and theoretical basis of instrumental analytical techniques – K_B.W12
W4: Explains the methodological basis and application of instrumental techniques, including spectroscopic, electrochemical, chromatographic, and mass spectrometry techniques – K_B.W12
W5: Knows and is able to apply the criteria for selecting an instrumental analytical method to perform a specific analytical task – K_B.W13
W6: Knows the definitions of analytical method validation parameters, is able to plan, perform, and evaluate the validation process – K_B.W14
W7: Knows the types of solutions and their classification according to various criteria (e.g., real solutions, colloidal solutions, suspensions) – K_B.W7
Learning outcomes - skills
U1: is able to optimize and validate a classical method for performing an analytical task – K_B.U7
U2: performs identification and quantitative analysis of elements and chemical compounds using appropriate classical methods – K_B.U8
U3: is able to select, optimize and validate an instrumental method for performing an analytical task – K_B.U7
U4: performs quantitative analysis of elements and chemical compounds using appropriate instrumental techniques – K_B.U8
U5: is able to assess the reliability and analytical quality of measurement results using appropriate statistical tools – K_B.U8
U6: performs analysis of water intended for pharmaceutical purposes using recommended analytical methods - K_B.U5
Learning outcomes - social competencies
K1: uses objective sources of information - K7
K2: is able to formulate conclusions from own measurements and observations - K8
Teaching methods
Lectures:
- informative lecture (conventional),
- problem-based lecture,
- multimedia presentation
Exercises (laboratory):
- methods: laboratory, observation, exercise,
Seminars:
- activating and problem-based methods – discussion,
- classic problem-based method,
- use of the Moodle platform
Expository teaching methods
- informative (conventional) lecture
- participatory lecture
- problem-based lecture
Exploratory teaching methods
- laboratory
- practical
- seminar
- experimental
Type of course
compulsory course
Prerequisites
To complete the subject, it is necessary to have basic knowledge about the properties of chemical compounds and chemical analysis, obtained as part of the implementation of the program of classes in general and inorganic chemistry. In addition, the student should have knowledge and skills acquired in the subjects of mathematics and statistics.
Course coordinators
Assessment criteria
Exam: W1-W7, U1-U6
Laboratories: W2, W5, W6, W7, U2, U4, U5, U6
Classes: W1, W3, U1-U6
Activity: K1, K2
Practical placement
The education program does not provide for professional internships.
Bibliography
Additional information
Additional information (registration calendar, class conductors,
localization and schedules of classes), might be available in the USOSweb system: