Advanced methods of instrumental analysis 0600-S3-DSC-ZMAI

Laser ABLATION (LIBS) in chemical analysis. ICP MS method in analysisX-ray (XRF) applications in metals determination. Elelctron spectroscopy (XPS, Augera) in surface analysis. Elelctron microscopy in surface imaging. ( SEM, AFM)
FTIR imaging with focal plane detection. Ramana spectra for identification of materials. Advanced NMR
spectra.
Laboratory
1.Interpretation of 1H NMR i 13C NMR COSY, NOE NOESY spectra.
2 Infrared spectroscopy measuremnts with confocal detection. for multicomponent analysis
3 Raman spectra with microscope imaging.

Total student workload

Contact hours with teacher - - participation in lectures - 15 h participation in laboratory- 15 h Self-study hours: preparation for laboratory – 20 hrs - preparation for test/ 25 h total: 75h (3ECTS)

Learning outcomes - knowledge

W1: has extended knowledge of chemical laws and its importance for science and humanity development - K_W01.X2A_W01 W2: Posseses knowledge and understanding on the basis of different analytical methods and their application in interpretation of analytical data - K_W09, X2A_W02, X2A_W04 W3: Is familiar with theoretical and practical aspects of quantitative analysis procedure by instrumental methods and is familiar with instrumentation performance K_W12, X2A_W05, X2A_W06 W4: Knows regulations of hygene and safety rules of work with in analytical laboratory, knows basic terms of toxicology; legal act concerning chemical laboratory work and hazardous materials, their storage and labeling _W12, X2A_W05, X2A_W06

Learning outcomes - skills

U1: Is able to use the knowledge and perform measurements of the specific chemical data and to prepare the report from the physico-chemical experiments .–K_U01, X2A_U01, X2A_U02, X2A_U04 U2: Is able to do quantitative analyses using instrumental methods and analytical procedures and prepare the analytical report ….– K_U05; X2A_U01, X2A_U02, X2A_U03, X2A_U01, X2A_U02, X2A_U04 U3: Is able to react properly in the case of different hazardous situations e.g. fire, contanct with chemical reagents -K_U14; , X2A_U02

Learning outcomes - social competencies

K1: effectively works with large amount of informations and is able to find the correltaions between the phenomennons and properly preprare the conclusions according to the rules of logic .–K_K01, X2A_K01, X2A_U07 K1: K2: Professionalism and ethics: Knows and applies basics and standards of of chemistry employee, among others ethical; understand the social importance of the profession; importance of the intelectual honesty, is caring about health and natural environment in his activities and in social groups. K_K06, X2A_K03, X2A_K04

Teaching methods

Lecture: expository Lecture using multimedia presentations and elements of discussions. Tutorial – practical Laboratorium: laboratory.

Observation/demonstration teaching methods

- display

Expository teaching methods

- problem-based lecture

Exploratory teaching methods

- laboratory
- case study

Online teaching methods

- content-presentation-oriented methods

Type of course

elective course

Prerequisites

Knowledge on instrumnetal analysis and spectroscopy on the master of science or other graduations forementioned in the admittion procedure for Ph D studies.

Course coordinators

Edward Szłyk

Assessment criteria

Lecture : No Exam list of attendance and assay on the subject from the scientific literature
laboratory: compulsory accepted analyses report student.
Criteria:
satisfactory 3
Student knows theretical bases of the analytical method and can describe the exercises done in the laboratory.

satisfactory plus 3+
Student knows and understand the theoretical bases of analytical methods and know rules and applied in praration of the analytical report.
good 4
Student knows and understand theoretical background undestand the procedure of analyses. Is able to plan the experiments , draw the conclusions and writ the report.
good plus 4+
Knowledge is complete and understand the method. Is able to solve the analytical problems without help form instructor.
very good 5
Knowledge is extended beyond the lecture program, can ifind the proper method of analysis in the library and applie it to the new problem.
n this block students acquire skills of sample preparation for analysis, calibration rules, checking of analytical instruments, running analyses, methods of results preparation using statistical analysis, writing reports according to good laboratory practices.

Practical placement

None.

Bibliography

1. Z. Kęcki, Podstawy spektroskopii molekularnej, PWN, W-wa 1992.
2. . J. Sadlej, Spektroskopia molekularna, WNT, W-wa 2002.
3. N.L. Alpert, W.E. Keiser, H.A. Szymański, Spektroskopia w podczerwieni teoria i praktyka, W-wa 1974, PWN
4. Literatura w Spectroscopy Europe on line

Additional information

Additional information (registration calendar, class conductors, localization and schedules of classes), might be available in the USOSweb system:

Description of 0600-S3-DSC-ZMAI in USOSweb