Ecoanalytics 0600-S2-PP/ACh-Eko

Lectures: 1. The importance of eco-analytics 2. Methods of collecting and testing air samples 3. Water testing methodologies 4. Isolation and determination of soil contamination 5. Classical and modern methods of collecting and preparing environmental samples 6. Modern trace analysis 7. Validation and calibration of the test method 8. Certified reference materials 9. Analysis of natural products - analytical aspects 10. Instrumental measurement techniques - applications in environmental analytics 11. Applications of chromatographic techniques in environmental analysis 12. Applications of spectroscopic techniques in environmental analysis 13. Applications of electrochemical techniques in environmental analysis 14. Applications of electromigration and other techniques in environmental analytics 15. Quality control systems

Lab:
Exercise 1 Thin layer chromatography (TLC, OP TLC) - determination of carboxylic acids
Exercise 2 Application of solid phase extraction (SPE) and thin layer chromatography (TLC) in the analysis of environmental samples Exercise 3 Determination of the hydrophobicity of parabens and their identification using liquid chromatography with spectrophotometric detection
Exercise 4 Determination of ibuprofen/ketoprofen residues in water by HPLC
Exercise 5 Determination of carbon content in soil - calibration, measurement methodology
Exercise 6 Gas Chromatography (GC) - determination of residues of organochlorine solvents
Exercise 7 Sample preparation methods - stationary phase microextraction (SPME)
Exercise 8 Electromigration techniques in qualitative and quantitative control

Total student workload

Hours with teacher: - participation in lectures - 15 hrs - participation in laboratories – 45 hrs - consultations – 15 hrs Self-study hours: - preparation of reports- 20 hrs - preparation for tests/ examination - 55 hrs

Learning outcomes - knowledge

Learning outcomes - skills

U01: apply theoretical knowledge in practice, including the use of facilities and other small laboratory equipment in a correct and proper way - K_U11. U02: do measurements - K_U11. U03: prepare for the tests, analytical procedures - K_U14. U04: can analyze, interpret and calculate the results obtained in the laboratory, in the course of his work - K_U11. U05: can develop analytical methodology - K_U14 U04: can analyze, interpret and calculate the results obtained in the laboratory, in the course of his work - K_U11. U05: can develop analytical methodology - K_U14

Learning outcomes - social competencies

K01: draws up research reports and notes that can be the basis for the preparation of a scientific publication - K_K07 K02: describes and compares the obtained test results with the standards (pattern libraries) and the available literature - K_K01, K_K02

Teaching methods

Lectures Laboratory classes

Expository teaching methods

- problem-based lecture

Exploratory teaching methods

- laboratory

Type of course

elective course

Prerequisites

General issues in the field of sample preparation methods and advanced chromatographic and electromigration techniques.

Course coordinators

Magdalena Ligor

Learning outcomes

W01: uses and explains terminology specific to the subject in English and its equivalent in Polish - K_W01
W02: recognizes and distinguishes between issues related to the subject of classes - K_W13, K_W14

U01: apply theoretical knowledge in practice, including the use of facilities and other small laboratory equipment in a correct and proper
way - K_U11.
U02: do measurements - K_U11.
U03: prepare for the tests, analytical procedures - K_U14.
U04: can analyze, interpret and calculate the results obtained in the laboratory, in the course of his work - K_U11.
U05: can develop analytical methodology - K_U14
U04: can analyze, interpret and calculate the results obtained in the laboratory, in the course of his work - K_U11.
U05: can develop analytical methodology - K_U14

K01: draws up research reports and notes that can be the basis for the preparation of a scientific publication - K_K07
K02: describes and compares the obtained test results with the standards (pattern libraries) and the available literature - K_K01, K_K02

Assessment criteria

To pass of laboratory classes is the knowledge of analytical procedures required for the correct execution of laboratory classes/experiments, analysis and positive evaluation of the colloquium, and report for each experiment – W01, W02, K02
fail - 2 pts (≥50%)
satisfactory - 3 pts (50-60%)
satisfactory plus - 3,5 pts (61-65%)
good - 4 pts (66-75%)
good plus - 4,5 pts (76-80%)
very good - 5 pts (≤81%)

Bibliography

Requested:
Scott R.P. W. , Tandem techniques, J. Wiley & Sons, New York 1998.
Poole C.F. , The Essence of Chromatography, Elsevier, Amsterdam 2003.
Recommended:
Namieśnik J., Chrzanowski W., New horizons and challenges in environmental analysis and monitoring. Centre of Excellence in Environmental Analysis and Monitoring, Gdańsk 2003
Pawliszyn J. [Ed.], Sampling and sample preparation for field and laboratory Elsevier Science B.V., Amsterdam 2002
Buszewski B., Dziubakiewicz M., Szumski M. [red.], Electromigration techniques, Theory and Practice, Springer, Berlin 2013.
Ardrey B., Liquid chromatography-mass spectrometry: an introduction, John Wiley & Sosns Inc., Chichester 2003.
Baranowska I., Buszewski B., Bioanalytics. Elsevier, Amsterdam 2022.
Buszewski B., Szultka M., Gadzała-Kopciuch R., Theory of extraction techniques, in: Comprehensive sampling and sample
preparation, J. Pawliszyn (ed.) Academic Press, New York 2012, str. 243-256.

Term 2023/24Z:

Term 2024/25Z:

Additional information

Additional information (registration calendar, class conductors, localization and schedules of classes), might be available in the USOSweb system:

Description of 0600-S2-PP/ACh-Eko in USOSweb