Advanced Instrumental Analysis 0600-S2-EN-AIA

Methods of Raman and IR spectroscopy in applications for quantitative analysis and identification.
Coupled chromatographic techniques with mass spectroscopy (ESI-MS, HPLC–ICP-MS). Application of laser ablation in chemical analysis.
Absorption and emission atomic spectroscopy (ASA, ICP, AES) and X-ray methods (XRF, XRD) used for determination of
metals in different matrices.
Electron spectroscopy (XPS, Auger) in surface analysis of materials.
Scaning electron microscopy (SEM, TEM, STEM) and atomic force microscopy (AFM) in applications for analysis of new materials.
Spectral imaging in IR spectroscopy (Focal IR with CCD).
Coupled analytical techniques in fine arts analysis.
Application of IR and Raman spectroscopy in biological material analysis.
Applications of XRF in forensic and food analysis..

Total student workload

Contact hours with teacher – 30 contact h: - participation in lectures - 30 h Self-study hours: - writing essays/ 30 h - reading literature- 15 h Altogether: 75 h (3ECTS)

Learning outcomes - knowledge

Student W1: Is familiar with the extended knowledge and understanding on instrumental methods of analysis - EK_W01. W2: . Knows newest achievements in the area of instrumental methods of analysis. EK_W02 W3: Is familiar with contemporary research techniques applied in instrumental methods of analysis. EK_W03

Learning outcomes - skills

U1. Is able to perform search in the scientific literature, is acquainted with the data bases in instrumental methods of analysis, is able to select informations in the literatures on the area of instrumental analysis EK_U02 U 2. Is able to solve the problems on instrumental methods of analysis using the proper techniques of analysis EK_U03 U3. Presents skills of continuous selfeducation in the area of instrumental methods of analysis. EK_U05

Learning outcomes - social competencies

K1. Presents active and responsible attitude to research, scientific initiative, understands problems of the academia environment EK_K01 K2. Is able to organize the team work, also interdisciplinary teams EK_K04

Teaching methods

Lecture: expository Lecture using multimedia presentations and elements of discussions

Prerequisites

Courses on analytical chemistry or instrumental analysis bacherol level

Course coordinators

Edward Szłyk

Assessment criteria

Lecture - K_W01, K_W02, K_W03,
Lecture: written essay on the chosen subject from the literature.

Practical placement

none

Bibliography

Literature basic
R. M. Silverstein. F. X. Webster, D.J. Kiemle , Spektroskopowe metody identyfikacji związków organicznych. WN. PWN
warszawa 2007.
2. Z. Kęcki, Podstawy spektroskopii molekularnej, PWN Warszawa, 1998r.
3. D.C. Harris Quantitative Chemical Analysis, W.H. Freeman and Co. N.Y. 8th Ed. 2010.
Literature additional
1. D. A. Skoog, D. M. West, F.J. Holler, S. R. Crouch, Podstawy Chemii Analitycznej. Tom. 1 i 2. WN. PWN Warszawa 2007

Additional information

Additional information (registration calendar, class conductors, localization and schedules of classes), might be available in the USOSweb system:

Description of 0600-S2-EN-AIA in USOSweb