Physico-chemical methods for characterizing materials 0600-S2-CKR-FMCM

Lecture
1. Classification and general characteristics of materials (natural and synthetic materials, inorganic and organic materials, ceramics, polymers, composites, metals and alloys, textiles, wood and paper).
2. Basic physicochemical properties of materials - morphology, microstructure, thermal properties, mechanical, optical, density, porosity, melting and boiling point, refractive index, viscosity, solubility, optical rotation.
3. Methods of determining the mechanical and optical properties of materials.
4. Methods for determining density, refraction index, melting point and boiling point.
5. Examination of material composition - elementary analysis (determination of the content of elements).
6. Chemical qualitative analysis of materials. Selected elements of analysis of inorganic substances (analysis of cations and anions in complex systems).
7. Selected elements of analysis of organic substances (methods of identification of functional groups in organic compounds).
8. Flame identification of polymeric materials
9. Color and color measurement of materials
10. Softening and flowing of amorphous plastics
11. Analysis of the degree of crystallinity of semicrystalline materials
12. Electrical conductivity of plastics
13. Methods of electrical conductivity measurement
14. Insulators and electrics - measurement of dielectric constant of insulating materials
15. New trends in polymer chemistry of electro-active materials

Lab
1. Determination of density of solids and liquids by hydrostatic balance, pycnometer and aerometer;
2. Determination of the melting point of organic substances using Boetius apparatus;
3. Determination of boiling point of organic substances during distillation;
4. Determination of the refractive index of a liquid by means of a refractometer;
5. Determination of solubility of selected inorganic and organic substances;
6. Determination of water content in solid samples;
7. Elemental analysis
8. Selected topics of chemical qualitative analysis - determination of inorganic substances in mixtures, analysis of functional groups in organic compounds;
9. Flame identification of plastics
10. Color determination of plastics
11. Softening temperature of thermoplastics according to Vicat method.
12. Densitometric titration of plastics.

Total student workload

1. Hours carried out with the participation of teachers: contact hours provided for in the study plan for a given subject (the sum of hours of all forms of classes in the subject), hours of individual consultations of a student / student / participant of the course: 85 2. Time devoted to individual work of a student / student / participant of the course needed to successfully complete the course, ie earlier preparation and completion of notes; collecting and selecting appropriate materials for classes, revision of the material required, writing works, projects, reading literature: 35 3. Time required to prepare for and to participate in the assessment process (e.g. exams), 30 150 godz.:25 h/ECTS =( 6 ECTS)

Learning outcomes - knowledge

W1: Graduate knowledge of the identification of various types of materials (inorganic, organic, polymeric compounds) using simple physicochemical methods - K_W01. W 2: Graduate knowledge of the chemical qualitative analysis of organic and inorganic compounds - K_W01. W3: Graduate knows the theoretical basis for measuring the color of materials - K_W01. W4: Graduate has knowledge of the softening and flowing of plastics - K_W01. W5: Graduate has knowledge of the degree of crystallinity of semicrystalline materials - K_W01. W6: He knows the basic information on the electrical conductivity of materials - K_W01. W7: Knows the methods of measuring electrical conductivity - K_W01. W8: Has basic information on insulators and electrets - K_W01. W9: Has a basic knowledge of contemporary trends in the chemistry of polymer electroactive materials. - K_W01.

Learning outcomes - skills

U1: Graduate has the ability to identify inorganic and organic compounds and determine their physical properties - K_U05. U2: Graduate has the ability to identify plastics using the flame and solvent methods - K_U05, K_U06 U3: Graduate can measure the color of materials - K_U05, U4: Graduate can independently measure the density of polyolefins by densitometric titration - K_U05, K_U06 U5: Graduate can determine the softening point according to Vicata - K_U05, U6: Graduate can determine the activation energy of electrical conductivity and interpret the result obtained. - K_U05, K_U06

Learning outcomes - social competencies

K1: Graduate can work independently and organize work effectively –K_K01 K2: Graduate sees the problem and can solve it - K_K05 K3: Graduate forms conclusions correctly - K_K05 K4: Graduate can work systematically and conscientiously - K_K06 K5: Graduate can work in a group- K_K02

Teaching methods

Lecture: Conventional lecture using multimedia techniques. Lab: Independent laboratory work, experiment method

Expository teaching methods

- discussion
- participatory lecture
- informative (conventional) lecture

Exploratory teaching methods

- experimental
- laboratory
- observation

Type of course

compulsory course

Prerequisites

Basic knowledge of general chemistry at the bachelor level

Course coordinators

Term 2022/23Z:

Halina Kaczmarek
Jacek Nowaczyk

Term 2025/26Z:

Kinga Mylkie
Jacek Nowaczyk
Ewa Olewnik-Kruszkowska

Term 2023/24Z:

Jacek Nowaczyk

Term 2024/25Z:

Kinga Mylkie
Jacek Nowaczyk
Ewa Olewnik-Kruszkowska

Assessment criteria

Lecture:oral exam

Laboratory: Final evaluation is the sum of the points obtained for the correct realization of experimental task and reports.

Practical placement

not applicable

Bibliography

1. Dereń J., Haber J., Pampuch R., Chemia ciała stałego, PWN, Warszawa 1975.
2. Dryński T., Ćwiczenia laboratoryjne z fizyki, PWN, Warszawa 1978.
3. Szydłowski H., Pracownia fizyczna wspomagana komputerem, PWN, Warszawa 2003.
4. Minczewski J. Marczenko Z., Chemia analityczna t.1 Podstawy teoretyczne i analiza jakościowa. PWN, Warszawa 2001.
5. Drożdż B., Analiza Organiczna , Kraków 2010 (http://web.archive.org/web/20110706013624/http://farmacja.cm-uj.krakow.pl/~mkz/ANALIZA_ORGANICZNA_2010.pdf)
6. Broniewski T., Kapko J., Płaczek W., Thomalla J., Metody badań i ocena właściwości tworzyw sztucznych, WNT, Warszawa 2000.
7. Przygocki W., Metody fizyczne badań polimerów, PWN, Warszawa 1990.
8. Brundle Richard C., Evans Charles A., Wilson Sham Jr., Encyclopedia of materials characterization BUTTERWORTH-HEINEMANN London 1992

Additional information

Additional information (registration calendar, class conductors, localization and schedules of classes), might be available in the USOSweb system:

Description of 0600-S2-CKR-FMCM in USOSweb