Thermal analysis
0600-S2-CKR-AT
Program contents of the lecture:
- Introduction to thermal analysis - basic concepts
- Phase transformations of the first and higher types - definition and examples
- Energy effects accompanying physical transformations and chemical reactions
- Factors affecting the measurement results in thermal analysis
- Procedures for collection and preparation of samples for analysis
- The division of thermoanalytical methods.
- Differential thermal analysis (definitions, apparatus, principle of measurement, applications)
- Thermogravimetry (definitions, apparatus, principle of measurement, applications)
- Differential scanning calorimetry (definitions, apparatus, principle of measurement, applications)
- Thermomechanical analysis (definitions, apparatus, measurement principle, applications)
- Coupled systems: TG-MS, TG-IR, TG-GC
Program contents of the laboratory:
- Introduction to thermal analysis - basic concepts
- Energy effects accompanying physical transitions and chemical reactions
- Factors affecting the measurements in thermal analysis
- Procedures for the collection and preparation of samples for analysis
- The division of thermoanalytical methods.
- Differential thermal analysis (definitions, apparatus, principle of measurement, applications)
- Thermogravimetry (definitions, apparatus, principle of measurement, applications)
- Differential scanning calorimetry (definitions, apparatus, principle of measurement, applications)
- Coupled systems - TG-IR, TG-MS.
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Term 2022/23Z:
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Term 2023/24Z:
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Term 2024/25Z:
Program contents of the lecture:
- Introduction to thermal analysis - basic concepts
- Phase transformations of the first and higher types - definition and examples
- Energy effects accompanying physical transformations and chemical reactions
- Factors affecting the measurement results in thermal analysis
- Procedures for collection and preparation of samples for analysis
- The division of thermoanalytical methods.
- Differential thermal analysis (definitions, apparatus, principle of measurement, applications)
- Thermogravimetry (definitions, apparatus, principle of measurement, applications)
- Differential scanning calorimetry (definitions, apparatus, principle of measurement, applications)
- Thermomechanical analysis (definitions, apparatus, measurement principle, applications)
- Coupled systems: TG-MS, TG-IR, TG-GC
Program contents of the laboratory:
- Introduction to thermal analysis - basic concepts
- Energy effects accompanying physical transitions and chemical reactions
- Factors affecting the measurements in thermal analysis
- Procedures for the collection and preparation of samples for analysis
- The division of thermoanalytical methods.
- Differential thermal analysis (definitions, apparatus, principle of measurement, applications)
- Thermogravimetry (definitions, apparatus, principle of measurement, applications)
- Differential scanning calorimetry (definitions, apparatus, principle of measurement, applications)
- Coupled systems - TG-IR, TG-MS. |
Term 2025/26Z:
Program contents of the lecture:
- Introduction to thermal analysis - basic concepts
- Phase transformations of the first and higher types - definition and examples
- Energy effects accompanying physical transformations and chemical reactions
- Factors affecting the measurement results in thermal analysis
- Procedures for collection and preparation of samples for analysis
- The division of thermoanalytical methods.
- Differential thermal analysis (definitions, apparatus, principle of measurement, applications)
- Thermogravimetry (definitions, apparatus, principle of measurement, applications)
- Differential scanning calorimetry (definitions, apparatus, principle of measurement, applications)
- Thermomechanical analysis (definitions, apparatus, measurement principle, applications)
- Coupled systems: TG-MS, TG-IR, TG-GC
Program contents of the laboratory:
- Introduction to thermal analysis - basic concepts
- Energy effects accompanying physical transitions and chemical reactions
- Factors affecting the measurements in thermal analysis
- Procedures for the collection and preparation of samples for analysis
- The division of thermoanalytical methods.
- Differential thermal analysis (definitions, apparatus, principle of measurement, applications)
- Thermogravimetry (definitions, apparatus, principle of measurement, applications)
- Differential scanning calorimetry (definitions, apparatus, principle of measurement, applications)
- Coupled systems - TG-IR, TG-MS. |
Total student workload
Lecture: 10 hours
Laboratory: 20 hours
Teacher consultation: 10 hours
Time devoted to individual student work: (preparation for classes, preparation for exams): 35 hours
Totale: 75 hours. (3 ECTS)
Learning outcomes - knowledge
W1: knows the basic concepts and laws applicable in the field of thermal analysis and the nomenclature related to the methods used - K_W01
W2: knows and understands the theoretical basis of the discussed thermal methods and is able to interpret the results of individual measurements in the form of numerical data or thermograms - K_W04
W3: knows the theoretical and practical aspects of conducting qualitative and quantitative analysis by thermal methods In the context of their use in forensic chemistry and the principles of operation of the apparatus - K_W06
W4: knows the regulations and rules of occupational safety and health, relating both to the handling of chemical reagents and the operation of measuring equipment - K_W016
Learning outcomes - skills
U1: has the ability to perform measurements using suitable apparatus and can process the results of thermal analysis measurements using relevant software- K_U05,
U2: is able to perform qualitative and quantitative analysis using thermal analysis methods on the basis of analytical procedures, prepare reports and critically discuss the results- K_U06
U3: is able to behave appropriately in case of, for example: fire, failure of apparatus or contact with chemical reagents- K_U16,
Learning outcomes - social competencies
K1: Analytical thinking: Independently and effectively works with results in the digital form or thermograms, notes the relationships between physical and chemical phenomena and correctly makes conclusions using the logic principles - K_K01,
K2: Professionalism and ethics: Knows and observes the rules and standards for a chemist, including ethical norms; understands and appreciates the importance of intellectual honesty, reliable processing and presentation of data; understands care for health and the environment. K_K08
Teaching methods
Marked below
Expository teaching methods
- informative (conventional) lecture
- participatory lecture
- problem-based lecture
Exploratory teaching methods
- project work
- seminar
- laboratory
Online teaching methods
- exchange and discussion methods
- integrative methods
- cooperation-based methods
Type of course
compulsory course
Prerequisites
Knowledge of chemistry and physics at the bachelor's level.
Course coordinators
Assessment criteria
Grading methods:
Lecture written exam in the form of answers to questions (2 hours); required threshold: for the grade sufficient -50%; sufficient plus - 61%; good- 66%; good plus 76%; very good above 80% W1, W2, W3, W4, U1, U2, U3, U4,
Laboratory pass: written tests 15 min before each class graded on a scale of 0-5; performance and passing of exercises based on prepared exercise reports and graded on a scale of 0-5pts; required threshold: for sufficient grade -50%; sufficient plus - 61%; good- 66%; good plus 76%; very good above 80% sum of points for tests and reports. W1, W2, W3, W4, U1, U2, U3, U4, U5.
Practical placement
Bibliography
Basic literature:
1. P.J. Haines, D. Kealey ¬– Instant Notes in Analytical Chemistry, 2022, Chemistry.Com.Pk.
2. P.J. Haines – Principles of Thermal Analysis and Calorimetry, Royal Society of Chemistry, Cambridge, 2002r. (online)
Supporting literature:
1) D.Schultze, Termiczna analiza różnicowa, PWN, W-wa, 1974r.
2) E. Pungor, A practical guide to instrumental analysis, CRC Press, Boca Raton, 2020.
3) G. Hellmiss, Thermal Analysis Methods in Forensic Science, Springer Science & Business Media, 2012r.
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Term 2022/23Z:
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Term 2023/24Z:
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Term 2024/25Z:
Basic literature:
1. P.J. Haines, D. Kealey ¬– Instant Notes in Analytical Chemistry, 2022, Chemistry.Com.Pk.
2. P.J. Haines – Principles of Thermal Analysis and Calorimetry, Royal Society of Chemistry, Cambridge, 2002r. (online)
Supporting literature:
1) D.Schultze, Termiczna analiza różnicowa, PWN, W-wa, 1974r.
2) E. Pungor, A practical guide to instrumental analysis, CRC Press, Boca Raton, 2020.
3) G. Hellmiss, Thermal Analysis Methods in Forensic Science, Springer Science & Business Media, 2012r.
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Term 2025/26Z:
Basic literature:
1. P.J. Haines, D. Kealey ¬– Instant Notes in Analytical Chemistry, 2022, Chemistry.Com.Pk.
2. P.J. Haines – Principles of Thermal Analysis and Calorimetry, Royal Society of Chemistry, Cambridge, 2002r. (online)
Supporting literature:
1) D.Schultze, Termiczna analiza różnicowa, PWN, W-wa, 1974r.
2) E. Pungor, A practical guide to instrumental analysis, CRC Press, Boca Raton, 2020.
3) G. Hellmiss, Thermal Analysis Methods in Forensic Science, Springer Science & Business Media, 2012r.
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Notes
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Term 2024/25Z:
Course on Moodle - login details during class.
https://moodle.umk.pl/WCh/course/view.php?id=39 |
Term 2025/26Z:
Course on Moodle - login details during class.
https://moodle.umk.pl/WCh/course/view.php?id=39 |
Additional information
Additional information (registration calendar, class conductors,
localization and schedules of classes), might be available in the USOSweb system: