Spectroscopic analysis 0600-S2-CKR-AS

Characteristics of electromagnetic radiation and basic types of molecular spectroscopy. Finding point groups for molecules based on their symmetry analysis. Introduction to the basic issues of group theory and the use of character tables to interpret electron and infrared spectra. UV-VIS chromophores, UV absorption bands of basic groups of organic compounds, fluorescence. Physical Basis of Nuclear Magnetic Resonance and Electron Paramagnetic Resonance. 1H, 13C, 15N NMR magnetic resonance spectroscopy. 2D NMR spectra. Introduction to mass spectrometry (ionization techniques, fragmentation process, relative peak intensities). Interpretation of simple mass spectrometry spectra. Using mass spectrometry to determine the molecular weight of a chemical compound and its molecular formula, determining the structure of a chemical compound based on the mass spectrum (various exercises).

Total student workload

Hours carried out with the participation of teachers (lecture, laboratory, consultations) 100 h. Individual students work 75 hours (preparation for the laboratory, preparing for the exam).

Learning outcomes - knowledge

The student will learn: basic concepts and research methods used in modern forensics, The student will learn the basic applications of molecular spectroscopy in chemistry, The student is familiar with the theoretical knowledge relating to the development of own analytical methodology using GC/MS

Learning outcomes - skills

The student will learn: basic concepts and research methods used in modern forensics, The student will learn the basic applications of molecular spectroscopy in chemistry, The student is familiar with the theoretical knowledge relating to developing their analytical methodology using GC/MS.

Learning outcomes - social competencies

The student independently and effectively works with a large amount of information, notices relationships between phenomena, and correctly draws conclusions using the principles of logic. He understands the importance of spectroscopic methods in modern forensics. It is focused on the continuous acquisition of new knowledge, skills, and experience; sees the need for continuous improvement and improvement of professional competencies; knows the limitations of their knowledge and understands the need for further education. Works systematically and has a positive approach to the difficulties standing in the way of achieving the set goal; meets deadlines; understands the need to systematically work on all projects. Fully independently pursues agreed goals, making independent and sometimes difficult decisions; can independently search for information in the professional literature.

Teaching methods

Exposing teaching methods - demonstration Didactic methods of administration - informative lecture (conventional), conversational lecture Searching teaching methods - exercise, laboratory, seminar.

Observation/demonstration teaching methods

- display

Expository teaching methods

- informative (conventional) lecture
- participatory lecture

Exploratory teaching methods

- seminar
- laboratory
- practical

Type of course

compulsory course

Prerequisites

Basic knowledge of chemistry and physics.

Course coordinators

Iwona Łakomska

Assessment criteria

Lecture – written exam (60%)
Laboratory – assessment credit – reports and colloquium (40%)

Practical placement

Not applicable

Bibliography

Basic Literature
1. Spektroskopowe metody identyfikacji związków organicznych - Silverstein R. M., Webster F. X., Kiemle D. J. PWN, 2007.
2. Z. Ruszkowski, Fizykochemia kryminalistyczna, Wydawnictwo CLK, Warszawa 1992
3. R. Bachliński, A. Policha (praca zbiorowa), Fizykochemiczne badania śladów kryminalistycznych, CLKP 2013.
4. A. Grodzicki, Symetria cząsteczek a ich widma oscylacyjne, PWN, 1988.
5. W. Zieliński, A. Rajca (praca zbiorowa), Metody spektroskopowe i ich zastosowanie do identyfikacji związków organicznych, WNT, 2000.
6. A. Cygański, Metody spektroskopowe w chemii analitycznej, WNT 2012.
7. Z. Kęcki, Podstawy spektroskopii molekularnej, PWN, 1992.
8. D. Kealey, P.J. Haines, Chemia analityczna. Krótkie wykłady, PWN, 2005.
9. E. de Hoffmann, J. Charette, V. Stroobant; tł. Leszek Konopski, Spektrometria mas, WNT, 1998.
10. R.A.W. Johnstone, M.E. Rose; z jęz. ang. tł. K. Bal, M. Daniewski, Spektrometria mas: podręcznik dla chemików i biochemików, PWN, 2001.
11. A.S. Płaziak Spektrometria mas związków organicznych Wydawnictwo Naukowe UAM, Poznań 1997
12. P. Sudera, J. Silberring, Spektrometria mas, Wydawnictwo Uniwersytetu Jagiellońskiego, 2006.
Supplementary Literature
1. H. Günther, NMR spectroscopy, Wiley, 1998.
2. A. Ejchart, L. Kozerski, Spektrometria magnetycznego rezonansu jądrowego 13C, PWN, 1981.
3. J. Sadlej, Spektroskopia molekularna,WNT, Warszawa 2002.
4. G.M. Barrow, Wstęp do spektroskopii molekularnej, PWN, Warszawa 1968.
5. T. Nowicka-Jankowska, E. Wieteska, K. Gorczyńska, A. Michalik, Spektrofotometria UV/VIS w analizie chemicznej, PWN, Warszawa 1988.
6. F.A. Cotton, Teoria grup; zastosowania w chemii, PWN, Warszawa 1973.
7. J.P. Simons, Fotochemia i spektroskopia, PWN, Warszawa 1976.
8. W. Henderson, J.S. McIndoe, Mass spectrometry of inorganic, coordination and organometallic compounds: tools, techniques, tips, Wiley, 2005.

Additional information

Additional information (registration calendar, class conductors, localization and schedules of classes), might be available in the USOSweb system:

Description of 0600-S2-CKR-AS in USOSweb