(in Polish) QuantChem – Zaawansowana analiza chemiczna materiałów 0600-S1-SP/W-QCh

Lecture:
Introduction to the techniques used: preparation of samples for analysis; isolation, separation and concentration of the analyte; measurement and measurement methods, analytical standards, device construction, device operation, health and safety rules, analysis errors, statistical evaluation of results.
Laboratory:
Advanced qualitative and quantitative analysis of chemical elements in raw materials, chemical industry products and environmental samples, using modern spectroscopic and physicochemical methods.
Study of the composition and physicochemical properties of solid and liquid materials using techniques such as: UV-Vis spectrophotometry, atomic absorption spectrometry (AAS), energy-dispersive X-ray fluorescence (EDXRF), particle size analysis, automatic viscometers (rotational and capillary) and total organic carbon (TOC) analyzer. The scope of the laboratory also includes comprehensive sample preparation.

Total student workload

1. 10 hours of lecture, 50 hours of laboratory, 5 hours of consultations, i.e. 65 contact hours, 2. 30 hours of individual work, 3. 30 h time required for preparation in the assessment process, 4. the total time of the student's workload is 125 hours. 125h:25h/ECTS= 5 ECTS

Learning outcomes - knowledge

W1: has in-depth knowledge of chemistry as a theoretical basis for learning analytical methods - K_W01, K_W15 W2: knows the basics of XRF, AAS and UV/VIS analyses, particle size measurement, TOC and statistical methods necessary for data processing - K_W06, K_W10 W3: knows and understands the risks and hazards associated with operating advanced research equipment - K_W16

Learning outcomes - skills

U1: is able to analyze and solve analytical problems - K_U01, K_U02 U2: is able to operate advanced research equipment - K_U05, K_U06, K_U12 U3: is able to develop and statistically evaluate experimental results - K_U05

Learning outcomes - social competencies

K1: is aware of the importance of acquired knowledge in scientific and professional work – K_K01, K_K05 K2: is able to properly prepare and conduct analysis of material - K_K02, K_K03 K3: knows and complies with the principles of occupational health and safety in the laboratory – K_K08

Teaching methods

Lecture: Conventional lecture with the use of multimedia presentations. Lab: Carrying out analysis independently, including preparing standards and samples and operating instrumental equipment and software.

Expository teaching methods

- problem-based lecture
- discussion
- informative (conventional) lecture
- participatory lecture

Exploratory teaching methods

- project work
- practical
- observation
- classic problem-solving
- laboratory
- experimental

Type of course

elective course

Prerequisites

Knowledge of general chemistry, analytical chemistry, and physical chemistry.

Course coordinators

Krzysztof Mazurek

Assessment criteria

Assessment criteria:

Lecture: Final work in the form of a paper or exam - W1, W2, U1, K1, K3.

Laboratory: continuous assessment (execution and passing reports on performed exercises, current preparation for classes and activity) - W2, W3, U2, U3, K2

The thresholds are assessed in accordance with the regulations of the NCU

Required thresholds for a satisfactory grade - 50-60%, sufficient plus - 61-65%, good 66-75%, good plus 76-81%, very good - 82-100%

Bibliography

Basic literature:
J. Minczewski, Z. Marczenko, Analytical chemistry, PWN, Warsaw 2005.
A. Cygański: Chemical methods of quantitative analysis. WNT, 4th edition, 2010
A. Cygański: Spectroscopic methods in analytical chemistry, WNT, 2009.
A. Cygański: Calculations in analytical chemistry. WNT, 2004.
P. Brouwer: Theory of XRF. PANalytical B.V., 2010.

Additional information

Additional information (registration calendar, class conductors, localization and schedules of classes), might be available in the USOSweb system:

Description of 0600-S1-SP/W-QCh in USOSweb