Elements analysis of medicinal products 0600-S1-CM-PW7a-APPL

Lecture:
Introduction to applied techniques: preparation of samples for analysis; separation, separation and concentration of the analyte; measurement and measurement methods; analytical standards; construction of the apparatus; operation of the apparatus; health and safety rules; analysis errors, statistical evaluation of results.
Lab:
Analysis of elements in medicinal products using the following methods: wet, UV/Vis, AAS, XRF. Analysis of liquid and solid samples. Preparation of samples for analysis. Physicochemical analysis of solid samples.

Total student workload

1. 10 hours of lecture, 35 hours of laboratory, 15 hours of consultations, i.e. 60 contact hours, 2. 20 hours of individual work, 3. 45 h time required for preparation in the assessment process, 4. the total time of the student's workload is 125 hours. 125h:25h/ECTS= 5 ECTS

Learning outcomes - knowledge

W1: has in-depth knowledge of chemistry as a theoretical basis for learning in the field of analytical methods - K_W01 W2: knows the basics of XRF, AAS and UV/VIS analyzes as well as statistical methods necessary for data processing - K_W02, K_W04 W3: knows and understands the risks and hazards associated with the operation of advanced research equipment - K_W09

Learning outcomes - skills

U1: can analyze and solve analytical problems - K_U01 U2: can operate advanced research equipment - K_U04 U3: can develop and statistically evaluate experimental results - K_U05

Learning outcomes - social competencies

K1: is aware of the importance of the acquired knowledge in scientific and professional work - K_K01 K2: can properly prepare and analyze the material - K_K03 K3: knows and observes the rules of occupational health and safety in the laboratory - K_K05

Teaching methods

Lecture: Conventional lecture with the use of multimedia presentations. Lab: Carrying out analysis independently, including preparing standards and samples and operating instrumental equipment and software.

Expository teaching methods

- informative (conventional) lecture
- participatory lecture
- problem-based lecture
- discussion

Exploratory teaching methods

- classic problem-solving
- project work
- practical
- laboratory
- observation
- experimental

Type of course

elective course

Prerequisites

Knowledge of general chemistry, analytical chemistry, and physical chemistry.

Course coordinators

Krzysztof Mazurek

Assessment criteria

Assessment criteria:

Lecture: Final work in the form of a paper, exam - W1, W2, U1, K3.

Laboratory: continuous assessment (execution and passing reports on performed exercises, current preparation for classes and activity) - W2, W3, U2, U3, K2

Classes: participation in classes - U1, K1

The thresholds are assessed in accordance with the regulations of the NCU

Required thresholds for a satisfactory grade - 50-60%, sufficient plus - 61-65%, good 66-75%, good plus 76-81%, very good - 82-100%

Bibliography

Basic literature:
J. Minczewski, Z. Marczenko, Analytical chemistry, PWN, Warsaw 2005.
A. Cygański: Chemical methods of quantitative analysis. WNT, 4th edition, 2010
A. Cygański: Spectroscopic methods in analytical chemistry, WNT, 2009.
A. Cygański: Calculations in analytical chemistry. WNT, 2004.
P. Brouwer: Theory of XRF. PANalytical B.V., 2010.

Additional information

Additional information (registration calendar, class conductors, localization and schedules of classes), might be available in the USOSweb system:

Description of 0600-S1-CM-PW7a-APPL in USOSweb