Fundamentals of analytical chemistry 0600-S1-CM-PCA
Lecture: Process of quantitative chemical analysis. Errors and statistical calculations of analytical results. Basic chemical laws used in quantitative analysis. Introduction to gravimetric determinations. Fundamentals of quantitative analysis in solution. Titrimetric analysis: acid-base, precipitations, redox, complexometric - EDTA. Titration analyses in applications. Theory of indicators: acid – base, redox, complexometric and precipitations (Mohr, Volhard, Fajans).
Calculus/ Tutorial:
Analytical calculations in analysis: alkacimetric, redoxometric, precipitation, gravimetric. Statistical calculations of analysis results.
Laboratory
Chemiacal analyses perfomed by students individually on: gravimetry deteremination of barium by precipitation of barium sulfate, titrations: alkacimetric of strong acid and base, weak acid i acetic acid, sodium bicarbonate, argetometric titrations of chlorides by MOhr method, bromides by Fajans method and thiocyanates by i Volhard method, redoximetric determination of oxalates, iron, and copper bz iodometric method, complexometric determination of calcium, magnesiu, and mixture of calcium and magnesium, prepartion of the standard solutions, of: acids, bases, KMnO4, sodium tiosulftae, silver nitrate, and EDTA, exercises indivdually performed by students.
Total student workload
Learning outcomes - knowledge
Learning outcomes - skills
Learning outcomes - social competencies
Teaching methods
Course coordinators
Assessment criteria
Lecture: exam written test 2,5h , open questions
Tutorial: Passed test on calculus
Lecture : Exam written test 2,5 h , open questions
Laboratory: 3 written tests, compulsory accepted analyses performed by student.
Criteria:
satisfactory 3
Student knows theretical bases of the analytical method and can describe the exercises done in the laboratory.
satisfactory plus 3+
Student knows and understand the theoretical bases of analytical methods and know rules and applied in praration of the analytical report.
good 4
Student knows and understand theoretical background undestand the procedure of analyses. Is able to plan the experiments , draw the conclusions and writ the report.
good plus 4+
Knowledge is complete and understand the method. Is able to solve the analytical problems without help form instructor.
very good 5
Knowledge is extended beyond the lecture program, can ifind the proper method of analysis in the library and applie it to the new problem.
Practical placement
None.
Bibliography
7. Wykaz literatury podstawowej:
1) D.C. Harris Quantitaive Chemical Analysis, VIIIth Ed. Freeman,and Co. N.Y.
2) A. Cygański Chemiczne metody analizy ilościowej WNT, Warszawa, 1992;
3) A. Hulanicki, Reakcje kwasów i zasad w chemii analitycznej, PWN, Warszawa, 1993;
4) E. Szłyk, M. Kurzawa, A. Szydłowska, A. Jastrzębska, Ilościowa Analiza Chemiczna. Metody wagowe i miareczkowe, UMK, 2005, Toruń:
8. Wykaz literatury uzupełniającej:
1) J. Minczewski, Z. Marczenko, Metody analityczne w analizie chemicznej. PWN Warszawa, 1998;
Additional information
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